DC Field | Value | Language |
dc.contributor.author | Hepokur, Ceylan | |
dc.contributor.author | Nursevin Öztop, H. | |
dc.contributor.author | Saraydin, Dursun | |
dc.date.accessioned | 2020-12-30T08:53:37Z | - |
dc.date.available | 2020-12-30T08:53:37Z | - |
dc.date.created | 2020-01-24 | |
dc.date.issued | 2020-01-24 | |
dc.identifier.citation | Hepokur C. Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin / Ceylan Hepokur, H. Nursevin Öztop, Dursun Saraydin // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 195–204. | |
dc.identifier.uri | https://ena.lpnu.ua/handle/ntb/55800 | - |
dc.description.abstract | Одержано полімери «з молекулярними відтисками» (молекулярно імпринтовані полімери, MIП) для
високоселективного розпізнавання серотоніну. Як мономери для
одержання МІП використано акриламід, метакрилову кислоту та
метакриламид. Проведено полімеризацію функціональних
мономерів з диметакрилатом етиленгліколю, діакрилатом 1,4-
бутандіолу і триметилпропантриакрилатом з серотоніном.
Видалення серотоніну з MIП проводили за допомогою суміші
метанол/оцтова кислота (4:1). Синтезовано неімпринтовані
полімери (НІП) без серотоніну. Одержані полімери досліджено за
допомогою методів Фур‘є-спектроскопії, диференційно скануючої
калориметрії, термогравіметричного аналізу та скануючої
електронної мікроскопії. Встановлено вплив температури, pH і
концентрації на адсорбцію серотоніну. Визначено значення
селективності таможливість повторного використання. | |
dc.description.abstract | Molecularly imprinted polymers (MIPs) were
prepared for highly selective recognition of serotonin.
Acrylamide, methacrylic acid and methacrylamide were
selected as the monomers for the production of MIPs.
Functional monomers were polymerized with ethylene
glycol dimethacrylate, 1,4-butanediol diacrylate, and
trimethylpropane triacrylate with serotonin (MIP-EGDMA,
MIP-BUT and MIP-TMT). Serotonin was removed from
MIP by the mixture of methanol/acetic acid (4:1). Nonimprinted polymers (NIPs) were synthesized without
serotonin (NIP-EGDMA, NIP-BUT and NIP-TMT). For
the characterization of synthesized polymers FTIR, DSC,
TGA, and SEM analysis were investigated. The parameters
that affect the adsorption of serotonin on polymers such as
temperature, pH and concentration were evaluated. The
selectivity and reusability studies were also investigated. | |
dc.format.extent | 195-204 | |
dc.language.iso | en | |
dc.publisher | Видавництво Львівської політехніки | |
dc.publisher | Lviv Politechnic Publishing House | |
dc.relation.ispartof | Chemistry & Chemical Technology, 2 (14), 2020 | |
dc.relation.uri | https://doi.org/10.1016/j.apsusc.2018.07.142 | |
dc.relation.uri | https://doi.org/10.1002/cbdv.200490069 | |
dc.relation.uri | https://doi.org/10.3390/ijms9122333 | |
dc.relation.uri | https://doi.org/10.1016/j.aca.2016.02.046 | |
dc.relation.uri | https://doi.org/10.3390/i7050155 | |
dc.relation.uri | https://doi.org/10.1016/j.bios.2017.08.022 | |
dc.relation.uri | https://doi.org/10.1016/j.aca.2005.01.052 | |
dc.relation.uri | https://doi.org/10.3176/proc.2018.2.04 | |
dc.relation.uri | https://doi.org/10.1016/j.elecom.2017.07.007 | |
dc.relation.uri | https://doi.org/10.1016/j.bios.2005.05.015 | |
dc.relation.uri | https://doi.org/10.1002/pola.20186 | |
dc.relation.uri | https://doi.org/10.1016/S0378-4347(99)00057-2 | |
dc.relation.uri | https://doi.org/10.1016/j.aca.2007.01.016 | |
dc.relation.uri | https://doi.org/10.1016/j.snb.2012.05.040 | |
dc.relation.uri | https://doi.org/10.1016/j.aca.2010.04.019 | |
dc.relation.uri | https://doi.org/10.1016/j.chroma.2006.09.065 | |
dc.relation.uri | https://doi.org/10.1002/macp.1987.021880408 | |
dc.relation.uri | https://doi.org/10.1016/j.talanta.2008.05.033 | |
dc.relation.uri | https://doi.org/10.1016/S0006-3495(96)79393-1 | |
dc.relation.uri | https://doi.org/10.1016/S1386-1425(02)00308-6 | |
dc.relation.uri | https://doi.org/10.1021/jp109337a | |
dc.relation.uri | https://doi.org/10.1016/S0142-9612(99)00048-4 | |
dc.relation.uri | https://doi.org/10.1002/pen.23950 | |
dc.relation.uri | https://doi.org/10.1016/j.talanta.2011.09.043 | |
dc.relation.uri | https://doi.org/10.1039/jr9600003973 | |
dc.relation.uri | https://doi.org/10.1007/s12221-017-7215-7 | |
dc.subject | акриламід | |
dc.subject | метакрилова кислота | |
dc.subject | метакриламід | |
dc.subject | молекулярно-імпринтовані полімери | |
dc.subject | серотонін | |
dc.subject | acrylamide | |
dc.subject | methacrylic acid | |
dc.subject | methacrylamide | |
dc.subject | molecularly imprinted polymers | |
dc.subject | serotonin | |
dc.title | Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin | |
dc.title.alternative | Одержання та характеристика полімерів з “молекулярними відтисками” для селективного розпізнавання серотоніну | |
dc.type | Article | |
dc.rights.holder | © Національний університет “Львівська політехніка”, 2020 | |
dc.rights.holder | © Hepokur C., Oztop N., Saraydin D., 2020 | |
dc.contributor.affiliation | Sivas Cumhuriyet University | |
dc.format.pages | 10 | |
dc.identifier.citationen | Hepokur C. Preparation and Characterization of Molecular Imprinted Polymer for the Selective Recognition of Serotonin / Ceylan Hepokur, H. Nursevin Öztop, Dursun Saraydin // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 2. — P. 195–204. | |
dc.identifier.doi | doi.org/10.23939/chcht14.02.195 | |
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dc.relation.referencesen | [2] Mathews C., van Holde K., Biochemistry: The Benjamin/Cummings Publ. Co., Redwood City, California 1990. | |
dc.relation.referencesen | [3] Sengupta B., Chaudhuri S., Banerjee A., Sengupta P., Chem. Biodivers., 2004, 1, 868. https://doi.org/10.1002/cbdv.200490069 | |
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dc.relation.referencesen | [5] Patra S., Roy E., Madhuri R., Sharma P., Anal. Chim. Acta, 2016, 918, 77. https://doi.org/10.1016/j.aca.2016.02.046 | |
dc.relation.referencesen | [6] Yan H., Row H., Int. J. Mol. Sci., 2006, 7, 155. https://doi.org/10.3390/i7050155 | |
dc.relation.referencesen | [7]JeCho S., Noh H., Won M. et al., Biosens. Bioelectron., 2018, 99, 471. https://doi.org/10.1016/j.bios.2017.08.022 | |
dc.relation.referencesen | [8] Hawkins D., Stevenson D., Reddy S., Anal. Chim. Acta, 2005, 542, 61. https://doi.org/10.1016/j.aca.2005.01.052 | |
dc.relation.referencesen | [9] Ayankojo A., Reut J., Öpik A. et al., Proceed. Estonian Acad. Sci., 2018, 67, 138. https://doi.org/10.3176/proc.2018.2.04 | |
dc.relation.referencesen | [10] Gálvez A., Mayorga-MatinezC., ParoloC. et al., Electrochem. Commun., 2017, 82, 6. https://doi.org/10.1016/j.elecom.2017.07.007 | |
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dc.relation.referencesen | [12] VazquezM., Spivak D.:J. Polym. Sci., 2004, 42, 3668. https://doi.org/10.1002/pola.20186 | |
dc.relation.referencesen | [13] Takeuchi T., Haginaka J.:J. Chromatogr. B, 1999, 728, 1. https://doi.org/10.1016/S0378-4347(99)00057-2 | |
dc.relation.referencesen | [14] Tooth B., Pap T., Horvath V., Horvai G., Anal. Chim. Acta, 2007, 591, 17. https://doi.org/10.1016/j.aca.2007.01.016 | |
dc.relation.referencesen | [15] Peeters M., Troost F., Van Grinsven B., et al., Sensor. Actuat. BChem., 2012, 172, 602. https://doi.org/10.1016/j.snb.2012.05.040 | |
dc.relation.referencesen | [16] Turiel E., Esteban A., Anal. Chim. Acta, 2010, 668, 87. https://doi.org/10.1016/j.aca.2010.04.019 | |
dc.relation.referencesen | [17] Urban J., Jandera P., Schoenmakers P.:J. Chromatogr. A, 2007, 1150, 279. https://doi.org/10.1016/j.chroma.2006.09.065 | |
dc.relation.referencesen | [18] Wulff G., Poll H.:Macromol. Chem. Phys., 1997, 188, 741. https://doi.org/10.1002/macp.1987.021880408 | |
dc.relation.referencesen | [19] Okutucu B.,Telefoncu A., Talanta, 2008, 76, 1153. https://doi.org/10.1016/j.talanta.2008.05.033 | |
dc.relation.referencesen | [20] Chattopathyay A., Rukmini R., Mukherjee S., Biophys. J., 1996, 71, 1952. https://doi.org/10.1016/S0006-3495(96)79393-1 | |
dc.relation.referencesen | [21] Ewing G., Instrumental Methods of Chemical Analysis, 4.edn. McGraw-Hill,Tokyo 1975. | |
dc.relation.referencesen | [22] Bayari S., Ide S., Spectrochim. Acta A, 2003, 59, 1255. https://doi.org/10.1016/S1386-1425(02)00308-6 | |
dc.relation.referencesen | [23] Lagutschenkov A., LangerJ., Berden G. et al.:J. Phys. Chem. A, 2010, 114, 13268. https://doi.org/10.1021/jp109337a | |
dc.relation.referencesen | [24] PenicheC., Argüelles-Monal W., Davidenko N. et al., Biomater., 1999, 20, 1869. https://doi.org/10.1016/S0142-9612(99)00048-4 | |
dc.relation.referencesen | [25] Işikver Y., Saraydin D., Polym. Eng. Sci., 2015, 55, 843. https://doi.org/10.1002/pen.23950 | |
dc.relation.referencesen | [26]Barati A., Kazemi E., Dadfarnia S., Shabani A.:JIEC, 2017, 46, 212. | |
dc.relation.referencesen | [27] Okutucu B.,Önal S., Talanta, 2011, 87, 74. https://doi.org/10.1016/j.talanta.2011.09.043 | |
dc.relation.referencesen | [28] Rudnick G., Kirk K., Fishkes H., Schuldiner S.:J. Biolog. Chem., 1989, 264, 14865. | |
dc.relation.referencesen | [29] Giles C., Macewan T., Nakhwa S., Smith D.:Journal of Chemical Society, 1960, 3973. https://doi.org/10.1039/jr9600003973 | |
dc.relation.referencesen | [30] Işikver Y., Fibers and Polymers, 2017, 18, 2070. https://doi.org/10.1007/s12221-017-7215-7 | |
dc.relation.referencesen | [31] Saraydin D., Karadağ E., Tr. J. Chem., 1996, 20, 234. | |
dc.citation.volume | 14 | |
dc.citation.issue | 2 | |
dc.citation.spage | 195 | |
dc.citation.epage | 204 | |
dc.coverage.placename | Львів | |
dc.coverage.placename | Lviv | |
Appears in Collections: | Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 2
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