https://oldena.lpnu.ua/handle/ntb/55776| Title: | The Intercalation Behaviour and Physico-Chemical Characterisation of Novel Intercalated Nanocomposite from Zinc/Aluminium Layered Double Hydroxides and Broadleaf Herbicide Clopyralid |
| Other Titles: | Інтеркаляційна поведінка і фізикохімічна характеристика нового інтеркальованого нанокомпозиту з подвійного гідроксиду цинку/алюмінію та клопіраліду з широколистяних гербіцидів |
| Authors: | Sharif, Sharifah Norain Mohd Hashim, Norhayati Isa, Illyas Md Mamat, Mazidah Ali, Noorshida Mohd Bakar, Suriani Abu Hussein, Mohd Zobir Mustafar, Suzaliza |
| Affiliation: | University Pendidikan Sultan Idris University Malaysia Terengganu University Putra Malaysia |
| Bibliographic description (Ukraine): | The Intercalation Behaviour and Physico-Chemical Characterisation of Novel Intercalated Nanocomposite from Zinc/Aluminium Layered Double Hydroxides and Broadleaf Herbicide Clopyralid / Sharifah Norain Mohd Sharif, Norhayati Hashim, Illyas Md Isa, Mazidah Mamat, Noorshida Mohd Ali, Suriani Abu Bakar, Mohd Zobir Hussein, Suzaliza Mustafar // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 1. — P. 38–46. |
| Bibliographic description (International): | The Intercalation Behaviour and Physico-Chemical Characterisation of Novel Intercalated Nanocomposite from Zinc/Aluminium Layered Double Hydroxides and Broadleaf Herbicide Clopyralid / Sharifah Norain Mohd Sharif, Norhayati Hashim, Illyas Md Isa, Mazidah Mamat, Noorshida Mohd Ali, Suriani Abu Bakar, Mohd Zobir Hussein, Suzaliza Mustafar // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2020. — Vol 14. — No 1. — P. 38–46. |
| Is part of: | Chemistry & Chemical Technology, 1 (14), 2020 |
| Issue: | 1 |
| Issue Date: | 24-Jan-2020 |
| Publisher: | Видавництво Львівської політехніки Lviv Politechnic Publishing House |
| Place of the edition/event: | Львів Lviv |
| DOI: | doi.org/10.23939/chcht14.01.038 |
| Keywords: | подвійний гідроксид цинку/алюмінію спільне осадження клопіралід інтеркаляція гербіцид zinc/aluminium layered double hydroxide co-precipitation clopyralid intercalation herbicide |
| Number of pages: | 9 |
| Page range: | 38-46 |
| Start page: | 38 |
| End page: | 46 |
| Abstract: | Методом спільного осадження одержані
нові нанокомпозити, що містять подвійний гідроксид
цинку/алюмінію інтеркальований клопіралідом (Zn/Al-LDHCP). За допомогою порошкової дифракції (PXRD)
підтверджено виникнення інтеркаляції. Встановлено, що
результати Фур'є спектроскопії та елементного аналізу
узгоджуються з результатами PXRD, та підтверджують
інтеркаляцію клопіраліду. За допомогою термічних методів
аналізу показано, що термічну стійкість нанокомпозиту є
вищою у порівнянні з чистим клопіралідом. Запропонована
хімічна формула нанокомпозиту [Zn0.75Al0.25 (OH) 2]
[C5H2Cl2NCOO] -0.250.67H2O та розраховано вміст
клопіраліду в Zn/Al-LDH (25,39 %). Приведені перспективи
використання нового нанокомпозиту Zn/Al-LDH-CP. This study reports on the preparation of novel zinc/aluminium layered double hydroxide intercalated clopyralid (Zn/Al-LDH-CP) nanocomposites fabricated via co-precipitation. An expansion of the interlayer gallery of Zn/Al-LDH for the accommodation of clopyralid was observed from the powder X-ray diffraction (PXRD) pattern, confirming the occurrence of intercalation. The results from Fourier transform infrared and elemental analysis were consistent with those from PXRD, thus supporting the intercalation of clopyralid. The thermal studies showed that the nanocomposite had better thermal stability compared to pristine clopyralid. Based on these data, the chemical formula of the nanocomposite was proposed as [Zn0.75Al0.25(OH)2][C5H2Cl2NCOO]- 0.250.67H2O, and the percentage loading of clopyralid in the interlayer gallery of Zn/Al-LDH was calculated to be 25.39 %. These characterisation results indicate a very promising future for this novel Zn/Al-LDH-CP nanocomposite. |
| URI: | https://ena.lpnu.ua/handle/ntb/55776 |
| Copyright owner: | © Національний університет “Львівська політехніка”, 2020 © Sharif S., Hashim N., Isa I., Mamat M., Ali N., Bakar S., Hussein M., Mustafar S., 2020 |
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| Appears in Collections: | Chemistry & Chemical Technology. – 2020. – Vol. 14, No. 1 |
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