| DC Field | Value | Language |
|---|
| dc.contributor.author | Pourbakhshi, Yasaman | |
| dc.contributor.author | Bahramy, Abdul Rahman | |
| dc.contributor.author | Shanha, Farshid Ghorbani | |
| dc.contributor.author | Assari, Mohammad Javad | |
| dc.contributor.author | Tajik, Leila | |
| dc.contributor.author | Farhadian, Maryam | |
| dc.date.accessioned | 2020-03-03T09:04:14Z | - |
| dc.date.available | 2020-03-03T09:04:14Z | - |
| dc.date.created | 2019-02-28 | |
| dc.date.issued | 2019-02-28 | |
| dc.identifier.citation | Development of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine / Yasaman Pourbakhshi, Abdul Rahman Bahramy, Farshid Ghorbani Shanha, Mohammad Javad Assari, Leila Tajik, Maryam Farhadian // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 4. — P. 482–488. | |
| dc.identifier.uri | https://ena.lpnu.ua/handle/ntb/46500 | - |
| dc.description.abstract | 2,5-Гександіон (2,5-ГД), основний метаболіт
н-гексану, був вилучений із зразків сечі з використанням
твердофазної мікроекстракції на основі холодного волокна
(CF-HS-SPME) та проаналізований за допомогою газової
хроматографії з детектором йонізації полум'я (GC-FID). Важливі параметри для підвищення ефективності сорбції волокна,
включаючи об'єм зразка, час екстракції та температуру,
оптимізовані за допомогою центрального композиційного
плану експерименту. Встановлено оптимальні умови, за яких
визначено межу чутливості та відносні стандартні відхилення. Показано, що розроблений метод є швидким, чутливим
та простішим у порівнянні із звичайними методами
кількісного аналізу 2,5-ГД у зразках сечі. | |
| dc.description.abstract | 2,5-Hexanedione (2,5-HD), the main
metabolite of n-hexane was extracted from urine samples
using cold fiber head space solid-phase microextraction
(CF-HS-SPME) based on thermoelectric cooling and
analyzed with gas chromatography equipped with a flame
ionization detector (GC-FID). Important parameters for
improved efficiency of fiber sorption including sample
volume, extraction time and temperature were optimized
using a central composite design. The optimum conditions
were determined, under which the detection limit and the
relative standard deviations were found. The method was
shown to be rapid, sensitive and easier than conventional
methods for quantitative analysis of 2,5-HD in urine samples. | |
| dc.format.extent | 482-488 | |
| dc.language.iso | en | |
| dc.publisher | Видавництво Львівської політехніки | |
| dc.publisher | Lviv Politechnic Publishing House | |
| dc.relation.ispartof | Chemistry & Chemical Technology, 4 (13), 2019 | |
| dc.relation.uri | https://doi.org/10.1177/0192623316638962 | |
| dc.relation.uri | https://doi.org/10.1016/j.etap.2005.12.010 | |
| dc.relation.uri | https://doi.org/10.1289/ehp.9245 | |
| dc.relation.uri | https://doi.org/10.1016/0378-4347(95)00029-I | |
| dc.relation.uri | https://doi.org/10.1016/0378-4347(95)00257-X | |
| dc.relation.uri | https://doi.org/10.1016/0021-9673(92)85092-8 | |
| dc.relation.uri | https://doi.org/10.1002/(SICI)1097-0231(19981015)12:19<1410::AID-RCM339>3.0.CO;2-M | |
| dc.relation.uri | https://doi.org/10.1016/S0003-2670(01)01082-0 | |
| dc.relation.uri | https://doi.org/10.1134/S1061934815100032 | |
| dc.relation.uri | https://doi.org/10.1186/s40201-014-0123-5 | |
| dc.relation.uri | https://doi.org/10.1080/00032719.2011.644736 | |
| dc.relation.uri | https://doi.org/10.1007/s10661-011-2434-7 | |
| dc.relation.uri | https://doi.org/10.1002/jssc.201400262 | |
| dc.relation.uri | https://doi.org/10.1002/jssc.201500975 | |
| dc.relation.uri | https://doi.org/10.1007/s10661-012-2914-4 | |
| dc.relation.uri | https://doi.org/10.1021/ac00097a007 | |
| dc.relation.uri | https://doi.org/10.1016/j.chroma.2006.10.092 | |
| dc.relation.uri | https://doi.org/10.1021/jf0613942 | |
| dc.relation.uri | https://doi.org/10.1002/jssc.200600333 | |
| dc.relation.uri | https://doi.org/10.1016/j.aca.2015.10.016 | |
| dc.relation.uri | https://doi.org/10.1002/ffj.1809 | |
| dc.relation.uri | https://doi.org/10.1016/j.chroma.2008.09.005 | |
| dc.relation.uri | https://doi.org/10.1515/pjct-2017-0041 | |
| dc.relation.uri | https://doi.org/10.1002/jssc.201201148 | |
| dc.relation.uri | https://doi.org/10.1590/S0100-40422007000400009 | |
| dc.relation.uri | https://doi.org/10.1016/S1570-0232(02)00036-3 | |
| dc.subject | зразки сечі | |
| dc.subject | 2 | |
| dc.subject | 5-гександіон | |
| dc.subject | холодне волокно | |
| dc.subject | твердофазна мікроекстракція | |
| dc.subject | н-гексан | |
| dc.subject | urine samples | |
| dc.subject | 2 | |
| dc.subject | 5-hexanedione | |
| dc.subject | cold fiber | |
| dc.subject | solid-phase microextraction | |
| dc.subject | n-hexane | |
| dc.title | Development of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine | |
| dc.title.alternative | Твердофазна мікроекстракція на основі холодного волокна для аналізу 2,5 гександіону в сечі | |
| dc.type | Article | |
| dc.rights.holder | © Національний університет „Львівська політехніка“, 2019 | |
| dc.rights.holder | © Pourbakhshi Y., Bahramy A., Shanha F., Assari M., Tajik L., Farhadian M., 2019 | |
| dc.contributor.affiliation | Hamadan University of Medical Sciences | |
| dc.format.pages | 7 | |
| dc.identifier.citationen | Development of Cold Fiber Head Space Solid-Phase Microextraction for Analysis of 2,5 Hexandion in Urine / Yasaman Pourbakhshi, Abdul Rahman Bahramy, Farshid Ghorbani Shanha, Mohammad Javad Assari, Leila Tajik, Maryam Farhadian // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 4. — P. 482–488. | |
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| dc.relation.referencesen | 1. Morgan D., JokinenM., Johnson C. et al., Toxicol. Pathol., 2016, 44, 763. https://doi.org/10.1177/0192623316638962 | |
| dc.relation.referencesen | 2. Woehrling E., Zilz T., ColemanM., Environ. Toxicol. Pharm., 2006, 22, 249. https://doi.org/10.1016/j.etap.2005.12.010 | |
| dc.relation.referencesen | 3. Carelli V., Franceschini F., Venturi S., et al: Environ. Health. Perspect., 2007, 115, 113. https://doi.org/10.1289/ehp.9245 | |
| dc.relation.referencesen | 4. American Conference of Governmental Industrial Hygienists. Threshold Limit Values for Chemical Substances and Physical Agents & Biliological Exposure Indices. Cincinnati OH, 2015. | |
| dc.relation.referencesen | 5. Van Engelen J., Kezic S., HaanW. et al., J. Chromatogr. B, 1995, 667, 233. https://doi.org/10.1016/0378-4347(95)00029-I | |
| dc.relation.referencesen | 6. Gori G., Bartolucci G., Sturaro A. et al., J. Chromatogr. B, 1995, 673, 165. https://doi.org/10.1016/0378-4347(95)00257-X | |
| dc.relation.referencesen | 7. Colombini M., Carrai P., Fuoco R., Abete C., J.Chromatogr. A, 1992, 592, 255. https://doi.org/10.1016/0021-9673(92)85092-8 | |
| dc.relation.referencesen | 8. Andreoli R., Manini P., Mutti A. et al., Rapid. Commun. Mass. Spectr.,1998, 12,1410. https://doi.org/10.1002/(SICI)1097-0231(19981015)12:19<1410::AID-RCM339>3.0.CO;2-M | |
| dc.relation.referencesen | 9. Konidari C., Stalikas C., KarayannisM., Anal. Chim. Acta, 2001, 442, 231. https://doi.org/10.1016/S0003-2670(01)01082-0 | |
| dc.relation.referencesen | 10. Attari S., Bahrami A., Shahna F., Heidari M., J. Anal. Chem., 2015, 70, 1192. https://doi.org/10.1134/S1061934815100032 | |
| dc.relation.referencesen | 11. Attari S., Bahrami A., Shahna F., Heidari M., J. Environ. Health Sci. Eng., 2014, 12, 1. https://doi.org/10.1186/s40201-014-0123-5 | |
| dc.relation.referencesen | 12. Zare Sakhvidi M., Bahrami A., Ghiasvand A. et al., Anal. Lett., 2012, 45, 375. https://doi.org/10.1080/00032719.2011.644736 | |
| dc.relation.referencesen | 13. Sakhvidi M., Bahrami A., Ghiasvand A. et al., Environ. Monit. Assess., 2012, 184, 6483. https://doi.org/10.1007/s10661-011-2434-7 | |
| dc.relation.referencesen | 14. Zeverdegani S., Bahrami A., RismanchianM., Shahna F., J. Sep. Sci., 2014, 37, 1850. https://doi.org/10.1002/jssc.201400262 | |
| dc.relation.referencesen | 15. Heidari M., Bahrami A., Ghiasvand A. et al., J. Sep. Sci., 2015, 38, 4225. https://doi.org/10.1002/jssc.201500975 | |
| dc.relation.referencesen | 16. Sakhvidi M., Bahrami A.,Ghiasvand A. et al., Environ. Monit. Assess., 2013, 185, 4933. . https://doi.org/10.1007/s10661-012-2914-4 | |
| dc.relation.referencesen | 17. Jalali M., ZareSakhvidi M., Bahrami A. et al., J. Res. Health Sci. 2016, 16, 153 | |
| dc.relation.referencesen | 18. Zhang Z., Pawliszyn J., Anal. Chem., 1995, 67, 34. https://doi.org/10.1021/ac00097a007 | |
| dc.relation.referencesen | 19. Carasek E., Cudjoe E., Pawliszyn J., J.Chromatogr. A, 2007, 5, 10. https://doi.org/10.1016/j.chroma.2006.10.092 | |
| dc.relation.referencesen | 20. Carasek E., Pawliszyn J., J. Agric. Food Chem., 2006, 54, 8688. https://doi.org/10.1021/jf0613942 | |
| dc.relation.referencesen | 21. Chen Y., Begnaud F., Chaintreau A., Pawliszyn J., J. Sep. Sci., 2007, 30, 1037. https://doi.org/10.1002/jssc.200600333 | |
| dc.relation.referencesen | 22. Ghiasvand A., Pirdadeh-beiranvandM., Anal. Chim. Acta, 2015, 900, 56. https://doi.org/10.1016/j.aca.2015.10.016 | |
| dc.relation.referencesen | 23. Ghiasvand A., Flavour Fragr., 2007, 22, 377. https://doi.org/10.1002/ffj.1809 | |
| dc.relation.referencesen | 24. Tajik L., Bahrami A.,Ghiasvand A., Shahna F., Chem Pap., 2017, 71, 1829. | |
| dc.relation.referencesen | 25. Haddadi S., Pawliszyn J., J. Chromatogr. A, 2009, 1216, 2783. https://doi.org/10.1016/j.chroma.2008.09.005 | |
| dc.relation.referencesen | 26. Tajik L., Bahrami A., Ghiasvand A., Ghorbani S., Pol. J. Chem. Technol., 2017, 19, 9. https://doi.org/10.1515/pjct-2017-0041 | |
| dc.relation.referencesen | 27. Pawliszyn J., Solid PhaseMicroextraction: Theory and Practice. Wiley, New York 1997. | |
| dc.relation.referencesen | 28. Merib J., Nardini G., Bianchin J. et al., J. Sep. Sci., 2013, 36, 2410. https://doi.org/10.1002/jssc.201201148 | |
| dc.relation.referencesen | 29. Konidari C., Stalikas C., KarayannisM., Anal. Chim. Acta, 2001, 442, 231. https://doi.org/10.1016/S0003-2670(01)01082-0 | |
| dc.relation.referencesen | 30. Nolasco D., Gusmao A., SiqueiraM., Quim. Nova, 2007, 30, 805. https://doi.org/10.1590/S0100-40422007000400009 | |
| dc.relation.referencesen | 31. Dos Santos C., Passarelli M., Nascimento E.., J. Chromatogr. B, 2002, 778, 237. https://doi.org/10.1016/S1570-0232(02)00036-3 | |
| dc.citation.issue | 4 | |
| dc.citation.spage | 482 | |
| dc.citation.epage | 488 | |
| dc.coverage.placename | Львів | |
| dc.coverage.placename | Lviv | |
| Appears in Collections: | Chemistry & Chemical Technology. – 2019. – Vol. 13, No. 4
|
