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  1. Електронний науковий архів Науково-технічної бібліотеки Національного університету "Львівська політехніка"
  2. Електронний архів Науково-технічної бібліотеки
  3. Вісники та науково-технічні збірники, журнали
  4. Chemistry & Chemical Technology
  5. Chemistry & Chemical Technology. – 2019. – Vol. 13, No. 1

putin IS MURDERER

Please use this identifier to cite or link to this item: https://oldena.lpnu.ua/handle/ntb/46426
Title: An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition
Other Titles: Оброблені мікрохвилями у відсутності розчинника магнітні наночастинки MgFe2O4 як ефективний каталізатор реакції Міхаеля
Authors: Bansal, Shobha
Singh, Prabal Pratap
Affiliation: G.L.A University
Bibliographic description (Ukraine): Bansal S. An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition / Shobha Bansal, Prabal Pratap Singh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 1. — P. 18–22.
Bibliographic description (International): Bansal S. An efficient solvent free microwave assisted MgFe2O4 magnetic nanoparticles catalyzed green protocol towards Michael addition / Shobha Bansal, Prabal Pratap Singh // Chemistry & Chemical Technology. — Lviv : Lviv Politechnic Publishing House, 2019. — Vol 13. — No 1. — P. 18–22.
Is part of: Chemistry & Chemical Technology, 1 (13), 2019
Issue: 1
Issue Date: 28-Feb-2019
Publisher: Видавництво Львівської політехніки
Lviv Politechnic Publishing House
Place of the edition/event: Львів
Lviv
Keywords: магнітні наночастинки MgFe2O4
реакція Міхаеля
гетерогенний каталізатор
MgFe2O4 MNP’s
Michael addition
heterogeneous catalyst
Number of pages: 5
Page range: 18-22
Start page: 18
End page: 22
Abstract: Досліджено магнітні наночастинки MgFe2O4 як ефективний каталізатор для синтезу продуктів за реакцією Міхаеля внаслідок оброблення мікрохвилями у відсутності розчинника заміщених халконів і β-нітро стиролів з електронними донорами, такими як малононітрил та етилціаноацетат. Показано, що магнітні наночастинки MgFe2O4 є кращими гетерогенними каталізаторами (10 мол. %) у порівнянні з відомими каталізаторами. Визначено, що за п’ять циклів роботи синтезований каталіза- ор не втрачає каталітичної активності.
MgFe2O4 magnetic nanoparticles were used as an efficient catalyst for the synthesis of Michael products by treating substituted chalcones and β-nitro styrenes with electron donar species like malononitrile and ethyl cyanoacetate in solvent free microwave conditions. In this study, we report that MgFe2O4 magnetic nanoparticles were the best heterogeneous catalyst with 10 mol% loading for synthesis of Michael products as compared to several reported catalysts. The reusability of MgFe2O4 nanoparticles was checked for 5 times without appreciable loss of catalytic activity.
URI: https://ena.lpnu.ua/handle/ntb/46426
Copyright owner: © Національний університет „Львівська політехніка“, 2019
© Bansal S., Singh P., 2019
URL for reference material: https://doi.org/10.1055/s-1976-24200
https://doi.org/10.1016/0040-4020(76)80016-6
https://doi.org/10.1055/s-1979-28668
https://doi.org/10.1021/jo00125a064
https://doi.org/10.1021/ol000170g
https://doi.org/10.1016/S0040-4020(00)00618-9
https://doi.org/10.1055/s-2004-815948
https://doi.org/10.1016/j.tetlet.2007.05.026
https://doi.org/10.1016/S0040-4039(00)01820-7
https://doi.org/10.1021/ja00035a048
https://doi.org/10.1021/jo000185s
https://doi.org/10.1002/0471264180.or010.03
https://doi.org/10.1039/jr9570001015
https://doi.org/10.1055/s-1982-30055
https://doi.org/10.1016/S0040-4039(00)74494-7
https://doi.org/10.1081/SCC-120015762
https://doi.org/10.1016/j.tetlet.2005.08.010
https://doi.org/10.1021/op034161+
https://doi.org/10.1081/SCC-120002689
https://doi.org/10.1002/chem.200600870
https://doi.org/10.1002/chir.20956
https://doi.org/10.1016/0040-4039(81)80178-5
https://doi.org/10.3987/COM-97-S(N)77
https://doi.org/10.1080/00397918808064000
https://doi.org/10.1016/S0040-4039(01)01237-0
https://doi.org/10.1016/S0040-4039(03)01198-5
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https://doi.org/10.1039/b908632c
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2. JungM., Tetrahedron, 1976, 32, 3. https://doi.org/10.1016/0040-4020(76)80016-6
3. Peters J: Synthesis, 1979, 5, 321 https://doi.org/10.1055/s-1979-28668
4. Galli C., Marotta E., Right P., Rosini G., J. Org. Chem., 1995, 60, 6624. https://doi.org/10.1021/jo00125a064
5. Hanessian S., Pham V., Org. Lett., 2000, 2, 2975. https://doi.org/10.1021/ol000170g
6. Sibi M., Manyem S., Tetrahedron, 2000, 56, 8033. https://doi.org/10.1016/S0040-4020(00)00618-9
7. Ballini R., Bosica G., Fiorini D., Gil M., Synthesis, 2004, 4, 605. https://doi.org/10.1055/s-2004-815948
8. Chandrasekhar S., Rambabu C., Shyamsundar T., Tetrahedron Lett., 2007, 48, 4683. https://doi.org/10.1016/j.tetlet.2007.05.026
9. Tomohiro T., Takuya K., Tsutomu I., Tetrahedron Lett., 2000, 41, 10229. https://doi.org/10.1016/S0040-4039(00)01820-7
10. Spande T., Garraffo H., EdwardsM. et al., J. Am. Chem. Soc., 1992, 114, 3475. https://doi.org/10.1021/ja00035a048
11. Taasu K., Mizutani S., Noguchi M. et al., J. Org. Chem., 2000, 65, 4112. https://doi.org/10.1021/jo000185s
12. Bergmann E., Ginsburg D., Pappo R., Org. React. 1959, 10, 179. https://doi.org/10.1002/0471264180.or010.03
13. DaveyW., Gwilt J., J. Chem. Soc., 1957, 1015. https://doi.org/10.1039/jr9570001015
14. Garcia-Raso A., Garcia-Raso J., Campaner B. et al., Synthesis, 1982, 12, 1037. https://doi.org/10.1055/s-1982-30055
15. Ganesh S., Sarkar A., Tetrahedron Lett., 1991, 32, 1085. https://doi.org/10.1016/S0040-4039(00)74494-7
16. Li T-J., Cui Y., Chen G-F. et al., Synth. Commun., 2003, 33, 353. https://doi.org/10.1081/SCC-120015762
17. Ye W-P., Xu J-Y., Tan C-T., Tan C-H., Tetrahedron Lett., 2005, 46, 6875. https://doi.org/10.1016/j.tetlet.2005.08.010
18. ZahouilyM., Bahlaodhuan B., Aadil M. et al., Org. Pro. Res. Develop., 2004, 8, 275. https://doi.org/10.1021/op034161+
19. Ma Y-M., Zhang Y-M., Synth. Commun., 2002, 32, 819. https://doi.org/10.1081/SCC-120002689
20. Meciarova M., Toma S., Chem. Eur. J., 2007, 13, 1268. https://doi.org/10.1002/chem.200600870
21. Gu H., Li J., Qu G. et al., Chirality, 2011, 23, 514. https://doi.org/10.1002/chir.20956
22. Rosnati V., Saba A., Salimbeni A., Tetrahedron Lett., 1981, 22, 167. https://doi.org/10.1016/0040-4039(81)80178-5
23. Toda F., Takumi H., Nagami M., Tanaka K., Hetrocycles, 1998, 47, 469. https://doi.org/10.3987/COM-97-S(N)77
24. Bram G., Sansoulet J., Galons H., MiocqueM., Synth. Commun., 1988, 18, 367. https://doi.org/10.1080/00397918808064000
25. Kim D., Huh S., Kim S., Tetrahedron Lett., 2001, 42, 6299. https://doi.org/10.1016/S0040-4039(01)01237-0
26. Dere R., Pal R., Patil P., SalunkheM., Tetrahedron Lett., 2003, 44, 5351. https://doi.org/10.1016/S0040-4039(03)01198-5
27. Loupy P., Top. Curr. Chem., 1999, 206, 153. https://doi.org/10.1007/3-540-48664-X_7
28. Rao H., Jothilingam S., J. Chem. Sci., 2005, 117, 323. https://doi.org/10.1007/BF02708445
29. Li J., Cui Y., Chen G. et al., Synth. Commun., 2003, 33, 353. https://doi.org/10.1081/SCC-120015762
30. Bansal S., Kumar Y., Pippal P. et al., New J. Chem., 2017, 41, 2668. https://doi.org/10.1039/P.6NJ03701A
31. Pippal P., Singh P., Orient. J. Chem., 2017, 33, 1736. https://doi.org/10.13005/ojc/330418
32. SharmaM., Singh P., Bharadwaj P., J. Mol. Catal. A: Chem., 2011, 342, 6. https://doi.org/10.1016/j.molcata.2011.04.016
33. Liang D., Xin X., Gao H. et al., Chem. Res. Chinese Univ., 2009, 25, 169.
34. Ying A., Chen X., Wu C. et al., Synth. Commun., 2012, 42, 3455. https://doi.org/10.1080/00397911.2011.584260
35. Guo H., Li J., Qu G. et al., Chirality, 2011, 23, 514. https://doi.org/10.1002/chir.20956
36. Shen Z., Gu D., Yang J., Ji S., Synth. Commun., 2011, 41, 851. https://doi.org/10.1080/00397911003707006
37. Mohammad R., Najmedin A., Elham A., Forogh E., J. Mol. Catal. A, 2008, 292, 44. https://doi.org/10.1016/j.molcata.2008.06.003
38. Shi J., WangM., He L. et al., Chem. Commun., 2009, 4711. https://doi.org/10.1039/b908632c
39. Sakthivel V., Kasi P., Ind. J. Chem. B., 2010, 49, 469.
Content type: Article
Appears in Collections:Chemistry & Chemical Technology. – 2019. – Vol. 13, No. 1

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